UNIV. NEWS. NORTH-CAUCAS. REG. TECHNICAL SCIENCES SERIES. 2016; 2: 102-106
http://dx.doi.org/10.17213/0321-2653-2016-2-102-106
FEATURES OF THE MORPHOLOGY OF THE NANOSIZED POWDERS OF IRON-COBALTO ALLOY
Bublikov Evgeni Iliоdorovich – Candidate of Technical Sciences, assistant professor, department «Alternativnaya energetika», Don State Technical University, Rostov-on-Don, Russia. E-mail: afarallazov@ gmail.comantonovs-rostov@mail.ru
Kolomiec Valeri Vasilevich – engineer, department «Physik», Platov South-Russian State Polytechnic University (NPI), Novocherkassk, Russia. E-mail: RA6LAM@mail.ru
Kulinich Vladimir Ivanovich – Candidate of Technical Sciences, assistant professor, department «Physik», Platov South-Russian State Polytechnic University (NPI), Novocherkassk, Russia. E-mail: Chiniluk@mail.ru
Lyalko Elena Sergeevna – senior lector, department «Physik», Platov South-Russian State Polytechnic University (NPI), Novocherkassk, Russia. E-mail: elena.lialko@yandex.ru
Naiden Vladimir Vasilevich – Candidate of Technical Sciences, assistant professor, department «Physik», Platov South-Russian State Polytechnic University (NPI), Novocherkassk, Russia.
Chertova Inna Alekseevna – senior lector, department «Physik», Platov South-Russian State Polytechnic University (NPI), Novocherkassk, Russia. E-mail: inneskamaks@mail.ru
Abstract
The aim of this work is to study the possibility of obtaining nanosized filamentary powders of alloys of metals of the iron group of a given size and shape. The results of experimental studies of the process of electrocrystallization in electrochemical double-layer system of filaments of an alloy of iron-cobalt. The conditions for obtaining nanopowders with different morphology. The model of particle growth of the alloy. On the basis of electron microscopic analysis produced a classification of filiform crystals grown at constant and pulsed currents. This method of obtaining powders has a number of advantages: availability of preparative and apparatus for performing synthesis, the ability to control the process of electrocrystallization, obtaining the necessary amount of powder of different shapes, not contaminated by impurities.
Keywords: electrocrystallization; nanopowder; whiskers; pulsating current; needle-like crystals.
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